the ayurvedic pharmacopoeia of india - ccras ( pdfdrive ) (830801), страница 25
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Apply 2, 5, 8,11, 14, 17 µl of solution on TLC plate and develop the plate a distance of to 8 cm usingacetone : n-hexane (3 : 7) as mobile phase. After development, dry the plate in a currentof hot air and scan in the TLC scanner at a wavelength of 338 nm. Note the peak area andprepare the calibration curve by plotting peak area vs concentration of piperine.Extract accurately weighed about 6 g powder of vatis in 100 ml of alcohol in a Soxhletapparatus for 6 h.
Filter the extract while hot and dry completely and weigh. Take 25 mgof extract in a volumetric flask and dissolve in a mixture of methanol : chloroform (1 : 1)and make up the volume to 25 ml. Apply 3 µl of the test solutions on TLC plate. Develop,dry and scan the plate as described in the proceeding paragraph for calibration curve ofpiperine.
Record area under the curve for a peak corresponding to piperine in the testsolution. Calculate the amount of piperine in the test solution from the calibration curveof piperine.Other requirements:Microbial Limits:Aflatoxins:Appendix 2.4.Appendix 2.7.Storage: Store in a cool place in tightly closed containers, protected from light andmoisture.Therapeutic uses: Kāsa (cough); Śvāsa (Asthma).Dose: 3 g per day – to be dissolved slowly in the mouth.KS$ĀRAGeneral Description:Ks$āra are alkaline substances obtained from the water soluble ash of the drugs ofplant origin.Method of Preparation:The drugs are cut into small pieces and dried well. The pieces are placed in anearthen pot and burnt to ash.
Water is added to the ash in the ratio of 6:1 and mixed well.This is allowed to settle down over night and leter strained through a piece of cloth. Thisprocess of straining may be done two or three times till a clear liquid is obtained. Thisliquid is then put in an iron or earthen vessel and heated over a moderate fire till waterevaporates completely, leaving a solid salty white substance known as Ks$āra.Ks$āras are white in colour and hygroscopic in nature therefore should be kept inair-tight bottles. These last indefinitely.APĀMĀRGA KS$ĀRA(AFI, Part-I, 10:2)Definition:Apāmārga ks$āra is an off-white alkaline preparation made with the ingredients in theFormulation composition given below.Formulation composition:1.2.Apāmārga API BhasmaJala APIAchyranthes asperaWaterPl.1 part6 partsMethod of Preparation:Take ingredients of pharmacopoeial quality.Cut whole plant of Apāmārga into small pieces and dry completely.
Burn to ash(Bhasma).Add 6 parts of water to the Bhasma, stir well and keep over night.Next morning decant the clear liquid and filter through a three-layered muslin cloth.Repeat the filtering process till a colourless filtrate is obtained. Transfer filtered materialto a stainless steel vessel and heat to evaporate the water. Collect ks$āra deposited asflakes from the bottom of the vessel and grind it to a fine powder.Pack it in tightly closed containers to protect from light and moisture.Description:Fine powder, passing through sieve number 100; hygroscopic, odour faint and tastesaline; freely soluble in water.Identification:An aqueous solution yields the reactions characteristic of sodium and potassium,Appendix5.2.12.Physico-chemical parameters:Loss on drying at 1100:Acid- insoluble ash:pH (10% aqueoussolution)Not more than 4 per cent,2.2.10.Not more than 1 per cent,2.2.4.10 to 11,AppendixAppendixAppendix 3.3.Assay:Sodium:5.2.9.Potassium:5.2.9.Iron:5.2.5.Not less than 4 per cent,AppendixNot less than 29 per cent,AppendixNot less than 1.2 per cent,AppendixStorage: Store in a cool place in tightly closed containers, protected from light andmoisture.Therapeutic uses: Gulma (Abdominal Lump); Udara-śūla (Pain in the abdomen);.
Graha´ī (malabsorption syndrome); Vi¾ūcikā (Gastro-enteritis with piercingpain); Alasaka (Intestinal atony); Ajīrn$a (Dyspepsia); Aruci (tastelessness);Ānāha (distention of abdomen due to obstruction to passage of urine andstool); Arśa (Piles); Śarkarā (gravel in urine); Aśmarī (Calculus); Kr$mi (Helminthiasis);Āntarvidradhi (Hernia); Śvāsa (Asthma).Dose: 125 to 500 mg daily in divided dose.Anupāna: Water.ARKA LAVA³A(AFI, Part-I, 10:1)Definition:Arka Lava´a is a preparation made with the ingredients in the Formulation compositiongiven below.Formulation composition:1.2.Arka patra APISaindhava lava´a APICalotropis proceraRock saltLf.1 part1 partMethod of Preparation:Take ingredients of pharmacopoeial quality.Collect mature Arka patra.
Place alternate layers of Arka patra and Saindhava lava´a inan earthen pot.Keep a śarāva to cover the pot. Seal the edge of the śarāva and the pot with sevenconsecutive layers of clay-smeared cloth and allow to dry.Subject it to fire till the pot becomes red-hot.
Remove the contents from the pot and grindto a fine powder in a khalva.Pack it in tightly closed containers to protect from light and moisture.Description:A fine powder, passing through sieve number 100; grey in colour, odourless, taste salty.Identification:An aqueous solution yields reactions characteristic of sodium, potassium, calcium,chloride and sulphate,Appendix 5.2.12.Physico-chemical parameters:Loss on drying at 1100:Acid- insoluble ash:pH (10% aqueous solution):Not more than 1 per cent,Not more than 3 per cent,9 to 10,Appendix 2.2.10.Appendix 2.2.4.Appendix 3.3.Assay:Sodium:5.2.9.Not less than 31 per cent,AppendixPotassium:5.2.9.Iron:5.2.5.Not less than 0.3 per cent,AppendixNot less than 0.11 per cent,AppendixStorage: Store in a cool place in tightly closed containers, protected from light andmoisture.Therapeutic uses: Gulma (Abdominal lump), Udara roga (diseases of abdomen),Plīhodara (Splenomegaly) Yak¨todara (enlargement of Liver).Dose: 1g daily in divided doses.Anupāna: Water, Butter milk.KALYĀ³AKA KS#ĀRA(AFI, Part-I, 10:6)Definition:Kalyā´aka ks$āra is a preparation made with the ingredients in the Formulationcomposition given below.Formulation composition:1.2.3.4.5.6.Śu´°hī APIMarica APIPippalī APISaindhava lava´a APISauvarchala lava´a APIVi²a lava´a API7.8.9.Harītakī APIBibhītakī APIĀmalakī API10.11.12.13.14.Dantī APIAru¾kara (Bhallātaka API)Citraka APISneha (Tila API)Mūtra (Gomūtra)Zingiber officinalePiper nigrumPiper longumRock saltBlack saltBlack salt(Official subsititute)Terminalia chebulaTerminalia belliricaPhyllanthus emblica(Emblica officinalis)Baliospermum montanumSemecarpus anacardiumPlumbago zeylanicaSesamum indicumCow’s urineRz.Fr.Fr.P.P.P.Rt.Fr.Rt.Oil1 part1 part1 part1 part1 part1 part1 part1 part1 part1 part1 part1 partQ.S.Q.S.Method of preparation:Take ingredients of pharmacopoeial quality.Clean, dry and powder the ingredients no.
1 to 10 and 12 separately and pass throughsieve number 85.Crush Bhallātaka in a khalva to a fine state.Mix all powdered ingredients. Levigate the above mixture with the Tila taila andGomūtra and prepare a homogeneous blend. Keep the homogeneous blend in an earthenpot and cover with a sarāva. Seal the edges of the pot by seven consecutive layers ofclay-smeared cloth and dry. Keep the pot on mild fire till it becomes red-hot.
Remove thecontent from the pot and grind to a fine powder.Pack it in tightly closed containers to protect from light and moisture.Description:Fine powder, passing through sieve number 100; hygroscopic, odour less, taste salty.Identification:i) An aqueous solution yields the reactions characteristic of sodium, potassium,carbonate, sulphate, chloride and bicarbonate,Appendix 5.2.12.ii) A solution in dilute hydrochloric acid gives reactions characteristic of calcium, andmagnesium,Appendix5.2.12.Physico-chemical parameters:Loss on drying at 1100:Not more than 6 per cent,2.2.10.Acid- insoluble ash:Not more than 1 per cent,2.2.4.pH (10% aqueous solution): 10 to 11,AppendixAppendixAppendix 3.3.Assay:Sodium:5.2.9.Potassium:5.2.9.Iron:5.2.5.Not less than 14 per cent,AppendixNot less than 2 per cent,AppendixNot less than 1.6 per cent,AppendixStorage: Store in a cool place in tightly closed containers, protected from light andmoisture.Therapeutic uses: Vibandha (Constipation), Ādhmāna (Flatulence), Gulma (Abdominallump), Udāvarta (upward movement of gases), Arśa (Piles), Pān#d#u (anaemia); Udararoga (diseases of abdomen); Kr#mi (Helminthiasis); Mūtrāghāta (Urinary obstruction);Aśmarī (Calculus); Śopha (oedema); Hr#droga (heart disease); Graha´ī (malabsorptionsyndrome); Meha (Excessive flow of urine); Plīharuja (pain due to splenic disease);Ānāha (distention of abdomen); Śvāsa (Asthma); Kāsa (cough); Agnimāndya (Digestiveimpairment).Dose: 1 g daily in divided doses.Anupāna: Gh¨ta.MŪLAKA KS$ĀRA(AFI, Part-I, 10:10)Definition:Mūlaka ks$āra is a powder preparation made with the ingredients in the Formulationcomposition given below.Formulation composition:1.2.Mūlaka API BhasmaJala APIRaphanus sativusWaterPl.1 part6 partsMethod of preparation:Take ingredients of pharmacopoeial quality.Collect mature Mūlaka, wash and cut into small pieces and dry completely.
Burn to ash(Bhasma).Add 6 parts of water to the Bhasma, stir well and keep overnight. Next morning decantthe clear liquid and filter through a three-layered muslin cloth. Repeat the filtering processtill a colourless filtrate is obtained. Transfer filtered material in to a stainless steel vesseland heat to evaporate the water. Collect ks$āra deposited as flakes from the bottom of thevessel and grind to a fine powder.Pack it in tightly closed containers to protect from light and moisture.Description: Fine powder, passing through sieve number 100; hygroscopic, odourless,taste salty; freely soluble in water.Identification:An aqueous solution yields the reactions characteristic of sodium and potassium,Appendix5.2.12.Physico-chemical parameters:Loss on drying at 1100:2.2.10.Acid- insoluble ash:2.2.4.pH (10% aqueous solution):Assay:Not more than 1 per cent,AppendixNot more than 1 per cent,Appendix10 to 11,Appendix 3.3.Sodium:5.2.9.Potassium:5.2.9.Iron:5.2.5.Not less than 4 per cent,AppendixNot less than 28 per cent,AppendixNot less than 2.2 per cent,AppendixStorage: Store in a cool place in tightly closed containers, protected from light andmoisture.Therapeutic uses: Mūtr#ak¨cchra (Dysuria); Aśmarī (Calculus); Gulma (Abdominallump); Vātavikāra (disorders due to vata do¾a).Dose: 1g daily in divided doses.Anupāna: Water.PALĀŚA KS$ĀRA(AFI, Part-I, 10:9)Definition:Palāśa ks$āra is a white alkaline preparation made with the ingredients in the Formulationcomposition given below.Formulation composition:1.2.Palāśa API-BhasmaJala APIButea monospermaWaterPl.1 part6 partsMethod of preparation:Take all ingredients of pharmacopoeial quality.Cut Palāśa into small pieces and dry completely.
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