the ayurvedic pharmacopoeia of india - ccras ( pdfdrive ) (830801), страница 27
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Stop heating and allow to stand overnight.Start heating on next day, stir and constantly check the Kalka by rolling between thefingers.Stop the heating when the kalka breaks down into pieces on attempting to form a varti(khara pāka lak¾ana), and at the appearance of froth over the oil. Expose the varti toflame and confirm the absence of crackling sound indicating absence of moisture.Filter while hot (about 800) through a muslin cloth and allow to cool.Pack it in tightly closed containers to protect from light and moisture.Description: A medicated oil, dark reddish brown in color with pleasant odour.Identification:Thin layer chromatography:Extract 2 g of the sample with 20 ml of alcohol at about 400 for 3 h. Cool, separate thealcohol layer and filter.
Concentrate to about 5 ml and carry out thin layerchromatography. Apply 10 µl of the extract on TLC plate. Develop the plate to a distanceof 8 cm using toluene : ethyl acetate : hexane (6 : 3 : 1) as mobile phase. Afterdevelopment, allow the plate to dry in air and spray with ethanol-sulphuric acid reagentfollowed by heating at 1100 for about 10 min.
It shows spots at Rf 0.71 (light brown),0.80 (light brown) and 0.88 (blackish.brown) under visible light.Physico-chemical parameters:Refractive index at 400:Weight per ml at 400:Saponification value:3.10.Iodine value:3.11.Acid value:3.12.Peroxide value:3.13.1.455 to 1.460,0.915 g to 0.930 g,180 to 195,Appendix 3.1.Appendix 3.2.Appendix80 to 100,AppendixNot more than 5,AppendixNot more than 5,AppendixAbsent,AppendixOther requirements:Mineral oil:3.15.Microbial Limits:Appendix 2.4.Aflatoxins:Appendix 2.7.Storage: Store in a cool place in tightly closed containers, protected from light andmoisture.Therapeutic uses: In conditions of Vāta-rakta (Gout) and(Hypertension), Śopha (oedema), Skandhagata Vāta (frozen shoulder).Dose: External application for Abhya¬ga.Raktagata-VātaDHĀNVANTARA TAILA(Syn.
Balā Taila)(AFI, Part-I, 8:22)Definition:Dhānvantara Taila is a liquid preparation made with the ingredients in the Formulationcomposition given below with Tila Taila as the basic ingredient.Formulation composition:1.Balā mūla (Balā API)Sida cordifolia2.Jala API for decoctionReduced toWater36.86 l4.61 l3.Payah (Godugdha API)Cow’s milk4.61 l4.Yava APIHordeum vulgare5.Kola APIKulattha APIBilva APIŚyonāka APIGambhārī APIPā°alā APIZizyphus jujubaDolichos biflorusAegle marmelosOroxylum indicumGmelina arboreaStereospermum suaveolens6.7.8.910.11.12.13.14.1516.Ga´ikārikā(Laghu Agnimantha API)Śālapar´ī APIP¨śnipar´ī APIB¨hatī APIKa´°akārī API19.Gok¾ura APIJala API for decoctionReduced toTaila (Tila API)Medā API20.Mahā Medā21.Dāru (Devadāru API)22.Ma®ji¾°ā APIKākolī17.18.23.24.K¾īra KākolīClerodendrum phlomidisDesmodium gangeticumUraria pictaSolanum indicumSolanum surattenseTribulus terrestrisWaterRt.4.61 kgSd.Fr.59.07 gSd.59.07 gSt.Bk.59.07 gSt.Bk.59.07 gSt.Bk.59.07 gSt.Bk.59.07 gSt.Bk.59.07 gPl.59.07 gPl.59.07 gRt.59.07 gRt.59.07 gFr.59.07 g59.07 g6.144 l768 mlOil768 mlRt.6gRt.6gHt.Wd.6gRt.6gWithania somniferaRt.6g(Official substitute)Withania somniferaRt.6gSesamum indicumAsparagus racemosus(Official substitute)Asparagus racemosus(Official substitute)Cedrus deodaraRubia cordifolia(Official substitute )2526.27.28.29.Candana (Rakta candana API)Śārivā (Śveta śārivā API)Ku¾°ha APITagara APIJīvaka30.§¾abhaka31.Saindhava lava´a APIKālānusārī (Tagara API)Śaileya APIVacā APIAgaru APIPunarnavā (Rakta punarnavā API)Aśvagandhā APIVarī (Śatāvarī API)K¾īraśukla (K¾īra Vidārī API)Ya¾°ī APIHarītakī APIĀmalakī API32.33.34.35.36.37.38.39.40.41.4243.44.45.46.47.48.Bibhītaka APIŚatāhvā APISūrpapar´i (Mā¾apar´ī API)Elā (Sūk¾mailā API)Tvak APIPatra (Tejapatra API)Pterocarpus santalinusHt.Wd.6gHemidesmus indicusRt.6gSaussurea lappaRt.6gValeriana wallichiiRt / Rz.6gPueraria tuberosa(Official substitute)Pueraria tuberosa(Official substitute)Rock saltRt.Tr.6gRt.Tr.6gValeriana wallichiiRz.6gParmelia perlataPl.6gAcorus calamusRz.6gAquilaria agallochaHt.Wd.6gBoerhaavia diffusaRt.6gWithania somniferaRt.6gAsparagus racemosusRt.Tr.6gIpomoea digitataRt.Tr.6gGlycyrrhiza glabraRt.6gTerminalia chebulaP.6gPhyllanthus emblica(Emblica officinalis)Terminalia belliricaP.6gP.6gAnethum sowaFr.6gTeramnus labialisPl.6gElettaria cardamomumSd.6gSt.Bk6gLf.6gCinnamomum zeylanicumCinnamomum tamala6gMethod of preparation:Take all ingredients of Pharmacopoeial quality.Wash and dry all the herbal raw materials thoroughly.Treat Tila taila to prepare Mūrchita Taila (Appendix 6.2.8.3).Pulverize the dried Balā mūla (kvātha dravya) to a coarse powder, add specified amountsof water, heat and reduce the volume to one eighth.
Filter with muslin cloth to obtain Balākvātha.Pulverize the dried ingredients numbered 4 to 16 (kvātha dravya) to coarse powder, addspecified quantity of water, heat and reduce the volume to one eighth. Filter with muslincloth to obtain kvātha.Take the other ingredients (kalka dravya) numbered 19 to 48 in the formulationcomposition, powder and pass through sieve number 85. Transfer the powderedingredients to a wet grinder and grind with sufficient quantity of water to prepare ahomogeneous blend (Kalka).Take Mūrchita Taila in a stainless steel vessel and heat it mildly.Add increments of Kalka. Stir thoroughly while adding the two ka¾āyā.Heat for 3 h with constant stirring maintaining the temperature between 500 and 900during the first hour of heating.
Stop heating and allow to stand overnight._____________________________________________________________________________Note: Stem bark of the ingredients number 7 to 11 of the formulation composition hasbeen used in place of root.Start heating next day, stir and constantly check the kalka by rolling between the fingers.Stop heating when the kalka breaks down into pieces on attempting to form a varti (kharapāka lak¾a´a), and at the appearance of froth over the oil. Expose the varti to flame andconfirm the absence of crackling sound indicating absence of moisture.Filter while hot (about 800) through a muslin cloth and allow to cool.Pack it in tightly closed containers to protect from light and moisture.Description:A medicated oil, redish brown in color with pleasant odour.Identification:Thin layer chromatography:Extract 2 g of the sample with 20 ml of alcohol at about 400 for 3 h. Cool, separate thealcohol layer and filter. Concentrate to 5 ml and carry out the thin layer chromatography.Apply 10 µl of the extract on TLC plate.
Develop the plate to a distance of 8 cm usingtoluene : ethyl acetate : hexane (6 : 3 : 1) as mobile phase. After development, allow theplate to dry in air and spray with ethanol-sulphuric acid reagent followed by heating at1100 for about 10 min. It shows spots at Rf 0.31 (light brown), 0.71 (brown), 0.83 (lightbrown) and 0.91 (blackish brown) under visible light.Physico-chemical parameters:Refractive index at 400:Weight per ml at 400:Saponification value:3.10.Iodine value:3.11.Acid value:3.12.Peroxide value:3.13.1.465 to 1.465,0.930 g to 0.940 g,180 to 195,Appendix 3.1.Appendix 3.2.Appendix100 to 120,AppendixNot more than 4,AppendixNot more than 5,AppendixAbsent,AppendixOther requirements:Mineral oil:3.15.Microbial Limits:Aflatoxins:Appendix 2.4.Appendix 2.7.Storage: Store in a cool place in tightly closed containers, protected from light andmoisture.Therapeutic uses: Vāta roga (diseases due to Vāta do¾a); Pak¾avadha (Hemiplegia);Sarvā¬ga vāta (Quadriplegia); Dhātu k¾aya (tissue wasting); Sūtikā roga .(Puerperal diseases) and Bāla roga (diseases of children).
External applicationforAbhya¬ga.Dose: Internally 6 to 12 ml daily in divided doses; as well as external application Q.S.GANDHARVAHASTA TAILA(AFI, Part-I, 8:12)Definition:Gandharvahasta Taila is a liquid preparation made with the ingredients in the Formulationcomposition described below with Tila Taila as the basic ingredient.Formulation composition:1.2.3.4.5.6.7.8.Gandharva hasta mūla (Era´²a API)Yava APINāgara (Śu´°hī API)Jala API for decoctionReduced toK¾īra (Godugdha API)Era´²a API -TailaGandharvahasta mūla (Era´²a API)Śu´°hī APIRicinus communisHordeum vulgareZingiber officinaleWaterCow’s milkRicinus communisRicinus communisZingiber officinaleRt.Sd.Rz.OilRt.Rz.4.8 k g3.07 kg96 g24.58 l6.14 l1.54 l768 g192 g48 gMethod of preparation:Take all ingredients of pharmacopoeial quality.Wash and dry all the herbal raw materials thoroughly.Treat Era´²a taila to prepare Mūrchita Era´²a Taila (Appendix 6.2.8.1).Pulverize the dried ingredients numbered 1 to 3 (kvātha dravya) to a coarse powder, addrequired amount of water, heat and reduce the volume to one fourth.
Filter with muslincloth to obtain kvātha. Take the other ingredients (kalka dravyas) numbered 7 and 8 ofthe formulation composition, dry, powder and pass through sieve number 85. Transfer thepowdered ingredients to wet grinder and grind with sufficient quantity of water to preparea homogeneous blend.Take Mūrchita Taila in a stainless steel vessel and heat it mildly.Add increments of Kalka. Stir thoroughly while adding the Kvātha and Godugdha.Heat for 3 h with constant stirring maintaining the temperature between 500 and 900during the first hour of heating. Stop heating and allow to stand overnight.Start the heating next day, stir and observe the boiling mixture for appearance of frothand constantly check the kalka for formation of varti (madhyama pāka lak¾a´a).Expose the varti to flame and confirm the absence of crackling sound indicating absenceof moisture. Stop heating when the kalka forms a varti and the froth appears.
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