the ayurvedic pharmacopoeia of india - ccras ( pdfdrive ) (830801), страница 28
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Filter whilehot (about 800) through a muslin cloth and allow to cool.Pack it in tightly closed containers to protect from light and moisture.Description:A medicated oil, yellowish brown in color with characteristic odour.Identification:Thin layer chromatography:Extract 2 g of the sample with 20 ml of alcohol at about 400 for 3 h. Cool, separate thealcohol layer and filter.
Concentrate to 5 ml and carry out the thin layer chromatography.Apply 10 µl of the extract on TLC plate. Develop the plate to a distance of 8 cm usingtoluene : ethyl acetate : hexane (6 : 3 : 1) as mobile phase. After development, allow theplate to dry in air and spray with ethanol-sulphuric acid reagent followed by heating at1100 for about 10 min. It shows spots at Rf 0.45 (light grey), 0.52 (grey), 0.75 (darkbrown) and 0.81 (dark brown) under visible light.Physico-chemical parameters:Refractive index at 400:Weight per ml at 400:Saponification value:3.10.Iodine value:3.11.Acid value:3.12.Peroxide value:3.13.1.451 to 1.460,0.975 g to 0.985 g,180 to 200,Appendix 3.1.Appendix 3.2.Appendix75 to 100,AppendixNot more than 4,AppendixNot more than 2,AppendixAbsent,AppendixOther requirements:Mineral oil:3.15.Microbial Limits:Aflatoxins:2.7.Appendix 2.4.AppendixStorage: Store in a cool place in tightly closed containers, protected from light andmoisture.Therapeutic uses: Vidradhi (abscess); Plīhā (enlargement of spleen); Gulma (abdominallump); Udāvarta (upward movement of gases); Śopha (oedema); Udara (diseases ofabdomen) and MahāVāta roga (major neurological disorders).Dose: 6 to12 ml daily in divided dosesAnupāna: Warm water.KO¯¯AMCUKK¡DI TAILA(AFI, Part-I, 8:10)Definition:Ko°°amcukkādi Taila is a liquid preparation made with the ingredients in the Formulationcomposition given below with Tila Taila as the basic ingredientFormulation composition:9.1.
Ko°°am (Ku¾°ha API)2. Cukku (Śu´°hī API)3. Vayambu (Vacā API)4. Śigru API5. Laśuna API6. Kārto°°i (Hi¼srā API)7. Devadruma (Devadāru API)8. Siddhārtha (Sar¾apa API)Suvahā (Rāsnā API)Saussurea lappaZingiber officinaleAcorus calamusMoringa oleiferaAllium sativumCapparis spinosaCedrus deodaraBrassica campestrisAlpinia galangaRt.Rz.Rz.St Bk.Bl.Rt.Ht.WdSd.21 g21 g21 g21 g21 g21 g21 g21 g(Official substitute)Rz.10.Oil11.milk12.Ci®cā rasa (Ci®cā API)21 gTilaja (Tila API)768 gDadhi (Godadhi API)Tamarindus indicaSesamum indicumCurd from cow’s768 gLf.3.07 lMethod of preparation:Take all ingredients of pharmacopoeial quality.Wash and dry all the herbal raw materials except ingredient 12 thoroughly.Treat Tila taila to prepare Mūrchita Taila (Appendix 6.2.8.3).Collect fresh leaves of ingredient number 12, wash thoroughly, grind and express svarasathrough muslin cloth.Take the other ingredients (kalka dravyas) with the exception of Laśuna and Sar¾apa,dry, powder and pass through sieve number 85.
Grind Laśuna . andSar¾apaseparately, add the powdered ingredients and grind withsufficient quantityof water to prepare a homogeneous blend. (Kalka)Take Mūrchita Taila in a stainless steel vessel and heat it mildly.Add increments of Kalka. Stir thoroughly while adding the Svarasa and Godadhi.Heat for 3 h with constant stirring maintaining the temperature between 50 and 900during the first hour of heating. Stop heating and allow to stand overnight.Start heating next day, stir and constantly check the Kalka by rolling between the fingers.Stop heating when the kalka breaks down into pieces on attempting to form a varti (kharapāka laksana), and at the appearance of froth over oil. Expose the varti to flame andconfirm the absence of crackling sound indicating absence of moisture.Filter while hot (about 800) through a muslin cloth and allow to cool.Pack it in tightly closed containers to protect from light and moisture.Description:A medicated oil, colour reddish brown, odour faint.Identification:Thin layer chromatography:Extract 2 g of the sample with 20 ml of alcohol at about 400 for 3 h.
Cool, separate thealcohol layer, filter, concentrate to 5 ml and carry out the thin layer chromatography.Apply 10 µl of the extract on TLC plate and develop the plate to a distance of 8 cm usingtoluene : ethyl acetate : hexane (6 : 3 : 1) as mobile phase. After development, allow theplate to dry in air and spray with ethanol-sulphuric acid reagent followed by heating1100 for about 10 min.
It shows spots at Rf 0.32 (light grey), 0.44 (light grey), 0.53 (lightgrey), 0.71 (brown), and 0.80 (brown) under visible light.Physico-chemical parameters:Refractive index at 400:Weight per ml at 400:Saponification value:3.10.Iodine value:3.11.Acid value:3.12.Peroxide value:3.13.1.461 to 1.463,0.920 to 0.940 g,150 to 175,Appendix 3.1.Appendix 3.2.Appendix75 to 100,AppendixNot more than 8,AppendixNot more than 4,AppendixAbsent,AppendixOther requirements:Mineral oil:3.15.Microbial Limits:Aflatoxins:Appendix 2.4.Appendix 2.7.Storage: Store in a cool place in tightly closed containers, protected from light andmoisture.Therapeutic uses: Āmavāta (Rheumatism); Vāta roga (disorders due to Vāta do¾a) andAngastambha (stiffness of body); External application for Abhya´ga.¾K ĪRABALĀ TAILA(AFI, Part-I, 8:11)Definition:K¾īrabalā taila is a liquid preparation made with the ingredients in the Formulationcomposition given below with Tila Taila as the basic ingredient.Formulation composition:1.parts2.3.4.5.partsBalā ka¾āya (Balā API)Sida cordifoliaRt.16Balā Kalka (Balā API)Taila API (Tila)K¾īra (Godugdha API)Jala APISida cordifoliaSesamum indicumCow’s milkWaterRt.Ol.1 part4 parts4 parts16Method of preparation:Take all ingredients of pharmacopoeial quality.Wash and dry Balā thoroughly.Treat Tila taila to prepare Mūrchita Taila.
(Appendix 6.2.8.3).Pulverize the dried Balā mūla (Kvātha dravya) to a coarse powder, add specified quantityof water, heat and reduce the volume to one fourth. Filter with muslin cloth to obtain Balākvātha.Take the ingredient (Kalka dravya) numbered 2 in the formulation composition, wash,dry, powder and pass through sieve number 85.
Transfer the powdered ingredient to wetgrinder and grind with sufficient quantity of water to prepare a homogeneous blend.(Kalka)Take Mūrchita Taila in a stainless steel vessel and heat it mildly.Add increments of Kalka. Stir thoroughly while adding the ka¾āya, Godugdha and water.Heat for 3 h with constant stirring maintaining the temperature between 500 and 900during the first hour of heating. Stop heating and allow to stand overnight.Start heating next day, stir and constantly check the Kalka by rolling between the fingers.Stop heating when the kalka breaks down into pieces on attempting to form a varti (kharapāka lak¾a´a), and at the appearance of froth over the oil. Expose the varti to flame andconfirm the absence of crackling sound indicating absence of moisture.
Filter while hot(about 800) through a muslin cloth and allow to cool.Pack it in tightly closed containers to protect from light and moisture.Description:A medicated oil, dark brown in color with pleasant odour.Identification:Thin layer chromatography:Extract 2 g of the sample with 20 ml of alcohol at about 400 for 3 h. Cool, separate thealcohol layer, filter, concentrate to 5 ml and carry out the thin layer chromatography.Apply 10 µl of the extract on TLC plate and develop the plate to a distance of 8 cm usingtoluene : ethyl acetate : hexane (6 : 3 : 1) as mobile phase. After development, allow theplate to dry in air and spray with ethanol-sulphuric acid reagent followed by heating at1100 for about 10 min.
It shows spots at Rf 0.42 (brown), 0.57 (brown), 0.70 (grey) and0.80 (light grey) under visible light.Physico-chemical parameters:Refractive index at 400:Weight per ml at 400:Saponification value:3.10.Iodine value:3.11.Acid value:3.12.Peroxide value:3.13.1.451 to 1.460,0.930 g to 0.945 g,185 to 200,Appendix 3.1.Appendix 3.2.Appendix75 to 100,AppendixNot more than 6.5,AppendixNot more than 2,AppendixAbsent,AppendixOther requirements:Mineral oil:3.15.Microbial Limits:Aflatoxins:Appendix 2.4.Appendix 2.7.Storage: Store in a cool place in tightly closed containers, protected from light andmoisture.Therapeutic uses: Vātarakta (Gout); Vāta roga (disorders due to Vāta do¾a); Śukra do¾a(Vitiation of ºukra dhatu); Rajo do¾a (Menstrual disorders); Kārśya (Emaciation);Svarabheda (hoarseness of voice). External application for Abhya¬ga, Nasya (nasaldrops), Pāna (oral use), Bastiprayoga (enema).Dose: 6 to 12 ml daily in divided doses.Anupāna: Warm water, milk.SAINDHAVĀDI TAILA(AFI, Part-I, 8:60)Definition:Saindhav¢di Taila is a liquid preparation made with the ingredients in the Formulationcomposition given below with tila taila as the basic ingredients.Formulation composition:1.g2.g3.g4.g5.g6.g7.g8.g9.3.07 lSaindhava lava´aRock salt28Arka APICalotropis proceraRt.28Marica APIPiper nigrumFr.28Jvalanākhya (Citraka) APIPlumbago zeylanicaRt.28Mārkava (Bh¨¬garāja) APIEclipta albaPl.28Haridrā APICurcuma longaRz.28Dāruharidrā APIBerberis aristataSt.28Tila taila APISesamum indicumOl.768Jala APIWaterMethod of preparation:Take all ingredient of pharmacopoeia quality.Treat tila taila is prepare Mūrchit tila taila.
(Appendix 6.2.8.3.)Wash, dry, powder the ingredients number 2 to 7 of the formulation composition (KalkaDravya) and pass through sieve number 85 to obtain fine powder. Transfer the powderedingredients to a wet grinder, add ingredient number 1 of the formulation composition andgrind with required amount of water to obtain a homogeneous blend (Kalka)Take Mūrchita taila in a stainless steel vessel and heat it mildly.Add increments of Kalka. Stir thoroughly while adding water. Heat for 3 h with constantstirring maintaining the temperature between 500 to 900 during the first hour of heating.Stop heating and allow to stand over night.Start heating next day, stir and constantly check the kalka by rolling between the fingers.Stop heating when the kalka breaks down in to pieces on attempting to form varti (Kharapaka lakshana) and at the appearance of froth over oil.
Expose the varti to flame andconfirm the absence of crackling sound indication absence of moisture.Filter while hot at about 800 through a muslin cloth and allow to cool.Pack it in tightly closed containers to protect from light and moisture.Description:Reddish yellow oily liquid, sticky to touch.Identification:Thin layer chromatography:Extract 25 ml of the formulation in a separatory funnel with methanol (20 ml x 3 ). Poolthe methanolic extracts, concentrate and make up the volume to 20 ml and carry out theThin Layer Chromatography.
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